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Rapid determination of 14 odorous compounds in drinking water using gas chromatography-mass spectrometry coupled with headspace solid-phase microextraction pretreatment

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成果类型:
期刊论文
作者:
Tong, Xuezhi;Zhang, Hao;Fan, Xiang;Yang, Shengyuan;Chen, Dongyang;...
通讯作者:
Yang, S.;Chen, D.
作者机构:
[Yang, Shengyuan; Tong, Xuezhi] Univ South China, Sch Publ Hlth, Hengyang Med Sch, Dept Publ Hlth Lab Sci, Hengyang 421001, Hunan, Peoples R China.
[Zeng, Dong; Feng, JiaLi; Fan, Xiang; Zhang, Hao; Chen, Dongyang] Hunan Prov Ctr Dis Control & Prevent, Changsha 410005, Hunan, Peoples R China.
[Tan, Shan] Changsha Med Univ, Sch Publ Hlth, Dept Gen Med, Changsha 410219, Hunan, Peoples R China.
通讯机构:
[Shengyuan Yang] D
[Dongyang Chen] H
Hunan Provincial Center for Disease Control and Prevention, Changsha, Hunan 410005, China<&wdkj&>Department of Public Health Laboratory Sciences, School of Public Health, Hengyang Medical School, University of South China, Hengyang, Hunan 421001, China
语种:
英文
期刊:
ANALYTICAL METHODS
ISSN:
1759-9660
年:
2022
卷:
14
期:
48
页码:
5076-5080
基金类别:
This work was financially supported by the Natural Science Foundation of Hunan Province, China (Grant No. 2021JJ70085), the National Institute of Environmental Health, the Chinese Center for Disease Control and Prevention (No. 2018shuifa25) and the Research Project of the Health Commission of Hunan Province (No. B2014134, No. B2016073, No. C20190035 and No. D202312069311).
机构署名:
本校为第一机构
院系归属:
公共卫生学院
摘要:
A sensitive and effective method was developed for the simultaneous determination of 14 odorous compounds in drinking water using gas chromatography-mass spectrometry (GC-MS) coupled with headspace solid phase microextraction (HS-SPME) pretreatment. The influencing factors including SPME fiber, ionic strength, temperature and time on the pretreatment procedure were evaluated systematically. Under the optimized conditions, 10 mL of the samples added with 1.0 g sodium chloride was extracted by CAR/PDMS fiber at 60 °C for 30 min and then desorbed...

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