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6π-Electrocyclization in water: microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones

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成果类型:
期刊论文
作者:
Li, Xiao-Yun;Liu, Yan;Chen, Xiao-Lan*;Lu, Xin-Yuan;Liang, Xing-Xing;...
通讯作者:
Chen, Xiao-Lan;Yu, Bing
作者机构:
[Li, Xiao-Yun; Liu, Yan; Chen, Xiao-Lan; Liang, Xing-Xing; Chen, XL; Yu, B; Qu, Ling-Bo; Lu, Xin-Yuan; Yu, Bing; Zhu, Shan-Shan] Zhengzhou Univ, Green Catalysis Ctr, Coll Chem, Zhengzhou 450001, Henan, Peoples R China.
[Liu, Yan] Xinyang Agr & Forestry Univ, Coll Biol & Pharmaceut Engn, Xinyang 464000, Peoples R China.
[Wei, Chuan-Wan] Univ South China, Sch Chem & Chem Engn, Hengyang 421001, Peoples R China.
通讯机构:
[Chen, XL; Yu, B] Z
Zhengzhou Univ, Green Catalysis Ctr, Coll Chem, Zhengzhou 450001, Henan, Peoples R China.
语种:
英文
期刊:
Green Chemistry
ISSN:
1463-9262
年:
2020
卷:
22
期:
14
页码:
4445-4449
基金类别:
We acknowledge the Center of Advanced Analysis & Computational Science (Zhengzhou University) and the financial support from the National Natural Science Foundation of China (21501010 and 21971224), Key Research Projects of Universities in Henan Province (20A150006, 20B350001), the Henan Province Young Talents Elevation Program (2019HYTP023), and Innovation and Entrepreneurship Training Program of Zhengzhou University (2019cxcy466).
机构署名:
本校为其他机构
院系归属:
化学化工学院
摘要:
Microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones through the annulation of ortho-heteroaryl anilines and CS2 was realized in water without using any catalysts and additives. The desired products were obtained in high yields through simple filtration. A remarkable E-factor of 0.45 and an EcoScale score of 85.5 were obtained....

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