Based on the fluorescence quenching effect produced by oxidation of acridine orange with BrO3- in the presence of KBr in a HC1 medium, a method for the determination of trace amount of BrOa in drinking water was proposed. Linear relationship between magnitude of decrease in fluorescence intensity (AF) and mass concentration of BrO3- was kept in the range of 10. 0--560. 0μg · L-1, when measured at (λex) 493 nm and (λem) 528 nm, Value of detection limit (3S/N) found was 3. 03 μg · L-1. The proposed method was applied to the determin...