The mild liquid-phase synthesis of 3-picoline from acrolein diethyl acetal and ammonia over heterogeneous catalysts

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作者信息关键词期刊信息会议信息基础信息归属信息摘要

成果类型：

期刊论文、会议论文

作者：

Luo, Cai-Wu*;Chao, Zi-Sheng;Lei, Bo;Wang, Hong;Zhang, Jun;...

通讯作者：

Luo, Cai-Wu

作者机构：

[Wang, Zheng-Hao; Luo, Cai-Wu; Wang, Hong; Lei, Bo; Zhang, Jun] Univ South China, Sch Environm & Safety Engn, Hengyang 421001, Hunan, Peoples R China.

[Luo, Cai-Wu; Wang, Hong; Lei, Bo] Hunan Engn Res Ctr Uranium Tailings Decommiss & T, Hengyang 421001, Hunan, Peoples R China.

[Chao, Zi-Sheng] Changsha Univ Sci & Technol, Coll Mat Sci & Engn, Changsha 410114, Hunan, Peoples R China.

通讯机构：

[Luo, Cai-Wu] U

[Luo, Cai-Wu] H

Univ South China, Sch Environm & Safety Engn, Hengyang 421001, Hunan, Peoples R China.

Hunan Engn Res Ctr Uranium Tailings Decommiss & T, Hengyang 421001, Hunan, Peoples R China.

语种：

英文

关键词：

Aldehydes;Ammonia;Batch reactors;Catalysts;Herbicides;Resins;3-picoline;H-ZSM-5;Heterogeneous catalyst;Influencing parameters;Liquid-phase synthesis;Reaction temperature;Ion exchange

期刊：

IOP Conference Series: Earth and Environmental Science

ISSN：

1755-1307

年：

2017

卷：

期：

页码：

012031

会议名称：

2017 3rd International Conference on Energy, Environment and Materials Science (EEMS)

会议论文集名称：

IOP Conference Series-Earth and Environmental Science

会议时间：

JUL 28-30, 2017

会议地点：

Northwestern Polytechnical University, Singapore, SINGAPORE

会议主办单位：

Northwestern Polytechnical University

会议赞助商：

Northwestern Polytechnical Univ, Nanyang Technological Univ

主编：

Wang, H

出版地：

DIRAC HOUSE, TEMPLE BACK, BRISTOL BS1 6BE, ENGLAND

出版者：

IOP PUBLISHING LTD

DOI：

10.1088/1755-1315/94/1/012031

基金类别：

This work was financially supported by the Educational Commission of Hunan Province (17C1361) and the Doctoral Scientific Research Foundation of University of South China (2016XQD36).

机构署名：

本校为第一且通讯机构

院系归属：

环境与安全工程学院

摘要：

The liquid-phase synthesis of 3-picoline from the reaction of acrolein diethyl acetal and ammonia over ion-exchanged resins (D402 and D002) and HZSM-5 (Si/Al = 25) was carried out in a batch reactor. Various influencing parameters, including by the addition of water, ion-exchanged resins, reaction temperature and HZSM-5, were systematically investigated. The results showed that the reaction could be directly conducted, and organic acid wasn't utilized. The highest yield of 3-picoline reached up to 24% using HZSM-5 as catalyst a...

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The mild liquid-phase synthesis of 3-picoline from acrolein diethyl acetal and ammonia over heterogeneous catalysts

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