Multilayer MXene (Ti3C2) with large layer spacing, large specific surface area, and few surface end-groups-F was obtained by using tetrapropylammonium hydroxide intercalation. The morphology, structure, and physicochemical properties of the samples were analyzed by characterization means of XRD, FT-IR, SEM, and BET, and the removal ability of the samples for uranyl ions was investigated by the batch removal experiments. The experimental results show that the removal of U(VI) by the intercalated Ti3C2 is more in line with the quasi-secondary kinetic model and Langmuir isothermal model, which is...