Electrocatalytic Cascade Selenylation/Cyclization/Deamination of 2‑Hydroxyaryl Enaminones: Synthesis of 3‑Selenylated Chromones under Mild Conditions

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成果类型：

期刊论文

作者：

Cen, Kaili;Liu, Yuan;Yu, Junhong;Zeng, Zhouting;Hou, Qian;...

通讯作者：

Cai, JH;Zhao, F;Wang, DH

作者机构：

[Cen, Kaili; Zeng, Zhouting; Cai, JH; Ouyang, Mixia; Cai, Jinhui; Wang, Qiaolin; He, Guojun; Yu, Junhong; Hou, Qian] Univ South China, Coll Chem & Chem Engn, Hengyang 421001, Hunan, Peoples R China.

[Liu, Yuan] Univ South China, Chuanshan Coll, Hengyang 421001, Hunan, Peoples R China.

[Zhao, Feng] Hunan Univ Med, Sch Pharmaceut Sci, Hunan Prov Key Lab Synthet Biol Tradit Chinese Med, Huaihua 418000, Hunan, Peoples R China.

[Wang, Dahan; Wang, DH] Shaoyang Univ, Dept Food & Chem Engn, Shaoyang 422100, Hunan, Peoples R China.

通讯机构：

[Cai, JH ] U

[Zhao, F ] H

[Wang, DH ] S

Univ South China, Coll Chem & Chem Engn, Hengyang 421001, Hunan, Peoples R China.

Hunan Univ Med, Sch Pharmaceut Sci, Hunan Prov Key Lab Synthet Biol Tradit Chinese Med, Huaihua 418000, Hunan, Peoples R China.

语种：

英文

期刊：

JOURNAL OF ORGANIC CHEMISTRY

ISSN：

0022-3263

年：

2024

卷：

期：

页码：

8632-8640

DOI：

10.1021/acs.joc.4c00567

基金类别：

National Natural Science Foundation of China [22301128]; Natural Science Foundation of China [2022JJ40353]; Natural Science Foundation of Hunan Province

机构署名：

本校为第一且通讯机构

院系归属：

化学化工学院

船山学院

摘要：

Herein, we disclosed a highly efficient pathway toward 3-selenylated chromone derivatives via electrocatalytic cascade selenylation/cyclization/deamination of 2-hydroxyaryl enaminones with diselenides. This method showed mild conditions, easy operation, wide substrate scope, and good functional group tolerance. Furthermore, this electrosynthesis strategy was amendable to scale-up the reaction. Additionally, the preliminary experiments revealed that this reaction probably ...

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Electrocatalytic Cascade Selenylation/Cyclization/Deamination of 2‑Hydroxyaryl Enaminones: Synthesis of 3‑Selenylated Chromones under Mild Conditions

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