期刊论文

Hu, AX

中文

有机化学

0253-2786

2004

24

8

902-905

10.3321/j.issn:0253-2786.2004.08.009

本校为其他机构

醇胺分别与2-溴-4′-甲氧基苯乙酮、2-溴-3′-氯苯丙酮、2-溴-4′-苄氧基苯基丙酮、2-溴-4′-苄氧基苯戊酮、6-甲氧基-2-溴乙酰基萘和6-甲氧基-2-(2-溴丙酰基)萘反应,合成相应的2-芳基-2-吗啉醇(产率80.7%～97.5%)及其盐酸盐.其结构经1H NMR,IR,MS确证.

2-Aryl-2-morpholinols were synthesized via the reactions of aminoalcohol with 2-bromo-4′-methoxyacetophenone, 2-bromo-4′-chloropropiophenone, 2-bromo-4′-benzyloxypropiophenone, 2-bromo-4′-benzyloxy- pentophenone, 6-methoxy-2-bromoacetylnaphthalene and 6-methoxy-2-(2- bromopropionyl) naphthalene by divergent synthetic method with yields of 80.7 %-97.5 % , respectively. The structures of 2-aryl-2-morpholinol...