Synthesis of bipolar tetradentate ligand and determination of fructose 1,6-diphosphate by resonance light scattering of its supramolecular polymer

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成果类型：

期刊论文

作者：

Li, Zhiyang;Xiao, Xilin*;Su, Changlin;Hu, Nan;Nie, Changming;...

通讯作者：

Liao, Lifu;Xiao, Xilin;Liu, Yong

作者机构：

[Su, Changlin; Liao, Lifu; Nie, Changming; Li, Zhiyang; Zhang, Di] Univ South China, Sch Chem & Chem Engn, Hunan Prov Key Lab Design & Applicat Actinide Com, Hengyang City 421001, Hunan, Peoples R China.

[Wang, Zhimei; Xiao, Xilin; Hu, Nan; Xiao, XL; Liu, Yong] Univ South China, Hunan Prov Engn Res Ctr Radioact Control Technol, Sch Resource & Environm & Safety Engn, Hengyang City 421001, Hunan, Peoples R China.

[Wang, Zhimei; Xiao, Xilin; Hu, Nan; Xiao, XL; Liu, Yong] Univ South China, Hunan Prov Engn Technol Res Ctr Uranium Tailings, Hengyang City 421001, Hunan, Peoples R China.

[Xiao, Xilin] Hunan Univ, State Key Lab Chemo & Biosensing & Chemometr, Changsha 410082, Hunan, Peoples R China.

通讯机构：

[Liao, Lifu; Xiao, XL; Liu, Y] U

[Xiao, Xilin] H

Univ South China, Sch Chem & Chem Engn, Hunan Prov Key Lab Design & Applicat Actinide Com, Hengyang City 421001, Hunan, Peoples R China.

Univ South China, Hunan Prov Engn Res Ctr Radioact Control Technol, Sch Resource & Environm & Safety Engn, Hengyang City 421001, Hunan, Peoples R China.

Univ South China, Hunan Prov Engn Technol Res Ctr Uranium Tailings, Hengyang City 421001, Hunan, Peoples R China.

语种：

英文

关键词：

Fructose 1,6-diphosphate;Bipolar tetradentate schiff base;Supramolecular polymer;Uranyl;Resonance light scattering

期刊：

Journal of Radioanalytical and Nuclear Chemistry

ISSN：

0236-5731

年：

2020

卷：

323

期：

页码：

431-438

DOI：

10.1007/s10967-019-06947-2

基金类别：

National Natural Science Foundation of China (NSFC)National Natural Science Foundation of China [11475079]; Defense Industrial Technology Development Program [JCKY2016403C001]; Hunan Provincial Natural Science Foundation of ChinaNatural Science Foundation of Hunan Province [2019JJ40244]; Key Project of Hunan Province Engineering Research Center of Radioactive Control Technology in Uranium Mining and Metallurgy [2018YKZX1007]; Key Project of Hunan Province Engineering Technology Research Center of Uranium Tailings Treatment [2018YKZX1007]

机构署名：

本校为第一且通讯机构

院系归属：

化学化工学院

摘要：

In this paper, a novel method was established for determination of fructose 1,6-diphosphate (F-1,6-BP) based on resonance light scattering (RLS), and a type of bipolar tetradentate schiff base H4L was synthesized. The study showed that under the optimization condition with the ligand concentration of 5 nmol mL(-1), pH 6.5, the reaction temperature of 25 degrees C, the reaction time of 30 min, RLS intensity had good linearity with the concentration of F-1,6-BP within the range of 0.4-5.0 nmol mL(-1), the limit of detection was 0.16 nmol mL(-1) and the relative standard deviation (RSD) was 1.83%...

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Synthesis of bipolar tetradentate ligand and determination of fructose 1,6-diphosphate by resonance light scattering of its supramolecular polymer

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