Direct electrochemical preparation of Ni-Zr alloy from mixture oxides in LiCl molten salt

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成果类型：

期刊论文

作者：

Ping, Xinyu;Liu, Kui;Liu, Yalan;Yuan, Liyong;Yao, Benlin;...

通讯作者：

Shi, Weiqun

作者机构：

[Yao, Benlin; Yuan, Liyong; Chai, Zhifang; Liu, Kui; Shi, Weiqun; Liu, Yalan; Ping, Xinyu] Chinese Acad Sci, Inst High Energy Phys, Lab Nucl Energy Chem, Beijing 100049, Peoples R China.

[Zhao, Xiuliang; Ping, Xinyu] Univ South China, Sch Nucl Sci & Technol, Hengyang 421000, Peoples R China.

[Yao, Benlin] China Inst Atom Energy, Dept Radiochem, Beijing 102413, Peoples R China.

[Chai, Zhifang] Soochow Univ, Sch Radiol & Interdisciplinary Sci, Suzhou 215123, Peoples R China.

通讯机构：

[Shi, Weiqun] C

Chinese Acad Sci, Inst High Energy Phys, Lab Nucl Energy Chem, Beijing 100049, Peoples R China.

语种：

英文

关键词：

Binary alloys;Chlorine compounds;Cyclic voltammetry;Electrolytic reduction;Intermetallics;Lithium alloys;Lithium compounds;Mixtures;Nickel;Nickel oxide;Pelletizing;Reduction;Sintering;Zirconium alloys;Zirconium compounds;Electrochemical preparation;Electrochemical reductions;Electrolysis process;Influence of process parameters;Nickel oxides (NiO);Oxide compositions;Preparation conditions;Voltammetry measurements;Nickel alloys

期刊：

JOURNAL OF THE ELECTROCHEMICAL SOCIETY

ISSN：

0013-4651

年：

2017

卷：

164

期：

页码：

D888-D894

DOI：

10.1149/2.1361713jes

基金类别：

We thank the support of the Science Challenge Project (JCKY2016212A504). We also thank the support of the National Natural Science Foundation of China (No. 21577144) and the Major Research Plan “Breeding and Transmutation of Nuclear Fuel in Advanced Nuclear Fission Energy System” of the Natural Science Foundation of China (91426302, 91326202).

机构署名：

本校为其他机构

院系归属：

核科学技术学院

摘要：

The Ni5Zr alloy prepared from the mixture of nickel oxide (NiO) and zirconium oxide (ZrO2) powders by direct electrochemical reduction was conducted in molten lithium chloride (LiCl) at 923 K. The electrochemical reduction behaviors of ZrO2 and NiO-ZrO2 mixture were firstly investigated by cyclic voltammetry measurements. The influence of process parameters such as oxide composition, compression force, sintering time, and cell voltage on the electrolysis process have been comprehensively evaluated in terms of the electrochemical reducibility of...

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Direct electrochemical preparation of Ni-Zr alloy from mixture oxides in LiCl molten salt

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