Metal‐Free C3 Hydroxylation of Quinoxalin‐2(1H)‐ones in Water

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作者信息关键词期刊信息基础信息归属信息摘要

成果类型：

期刊论文

作者：

Peng, Sha;Hu, Die;Hu, Jia-Li;Lin, Ying-Wu;Tang, Shan-Shan;...

通讯作者：

He, Wei-Min

作者机构：

[He, Wei-Min; Tang, Hai-Shan; Tang, Shan-Shan; Hu, Die; Hu, Jia-Li; Peng, Sha] Hunan Univ Sci & Engn, Dept Chem, Yongzhou 425100, Peoples R China.

[He, Wei-Min; He, Jun-Yi; Cao, Zhong] Changsha Univ Sci & Technol, Hunan Prov Key Lab Mat Protect Elect Power & Tran, Changsha 410114, Hunan, Peoples R China.

[Lin, Ying-Wu] Univ South China, Sch Chem & Chem Engn, Hengyang 421001, Peoples R China.

通讯机构：

[He, Wei-Min] H

[He, Wei-Min] C

Hunan Univ Sci & Engn, Dept Chem, Yongzhou 425100, Peoples R China.

Changsha Univ Sci & Technol, Hunan Prov Key Lab Mat Protect Elect Power & Tran, Changsha 410114, Hunan, Peoples R China.

语种：

英文

关键词：

hydroxylation;quinoxalin-2(1H)-one;in water;TPGS-750-M;green chemistry

期刊：

ADVANCED SYNTHESIS & CATALYSIS

ISSN：

1615-4150

年：

2019

卷：

361

期：

页码：

5721-5726

DOI：

10.1002/adsc.201901163

基金类别：

We are grateful for financial support from the Hunan Provincial Natural Science Foundation of China (No. 2019JJ20008).

机构署名：

本校为其他机构

院系归属：

化学化工学院

摘要：

A practical protocol for the preparation of quinoxaline-2,3(1H,4H)-diones through direct C(sp2)−H hydroxylation of quinoxalin-2(1H)-ones in recyclable DL-α-Tocopherol methoxypolyethylene glycol succinate solution (2 wt% in water) (TPGS-750-M/H2O) was developed. The target products were exclusively generated and could be collected through extraction and recrystallization. (Figure presented.). ©...

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Metal‐Free C3 Hydroxylation of Quinoxalin‐2(1H)‐ones in Water

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