In order to solve the problem of antimony(III) pollution in water environment, Fe-Mn layered double hydroxides (Fe-Mn LDH) were prepared by ultrasonic co-precipitation method, and the effects of initial pH, dosage, coexisting ions, adsorption time and temperature on the removal of antimony(III) from wastewater by Fe-Mn LDH were studied. The crystal structure, morphology and adsorption mechanism were characterized and analyzed by SEM, EDS, XRD, XPS and FTIR. The results show that the suitable conditions for antimony(III) removal are pH of 5, dos...