Base-free O-difluoromethylation of 1,3-diones with difluorocarbene

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成果类型：

期刊论文

作者：

Liu, Can;Deng, Xiao-Yun;Zeng, Xian-Liang;Zhao, Gang;Lin, Jin-Hong*;...

通讯作者：

Wang, Hongqing;Lin, Jin-Hong;Xiao, Ji-Chang

作者机构：

[Wang, Hongqing; Liu, Can] Univ South China, Sch Chem & Chem Engn, Hengyang 421001, Peoples R China.

[Zeng, Xian-Liang; Lin, Jin-Hong; Xiao, Ji-Chang; Lin, JH; Deng, Xiao-Yun; Zhao, Gang; Liu, Can] Univ Chinese Acad Sci, Chinese Acad Sci, Shanghai Inst Organ Chem, Key Lab Organofluorine Chem, 345 Lingling Rd, Shanghai 200032, Peoples R China.

通讯机构：

[Wang, Hongqing; Lin, JH; Xiao, JC] U

Univ South China, Sch Chem & Chem Engn, Hengyang 421001, Peoples R China.

Univ Chinese Acad Sci, Chinese Acad Sci, Shanghai Inst Organ Chem, Key Lab Organofluorine Chem, 345 Lingling Rd, Shanghai 200032, Peoples R China.

语种：

英文

关键词：

O-difluoromethylation;Difluorocarbene;Base-free;1,3-diones

期刊：

Journal of Fluorine Chemistry

ISSN：

0022-1139

年：

2016

卷：

192

页码：

27-30

DOI：

10.1016/j.jfluchem.2016.10.011

基金类别：

National Basic Research Program of ChinaNational Basic Research Program of China [2015CB931900, 2012CBA01200]; National Natural Science FoundationNational Natural Science Foundation of China (NSFC) [21421002, 21472222, 21502214, 11175080]; Chinese Academy of SciencesChinese Academy of Sciences [XDA02020105, XDA02020106]; Science and Technology Commission of Shanghai MunicipalityScience & Technology Commission of Shanghai Municipality (STCSM) [15DZ1200102, 14ZR1448800]; Natural Science Foundation of Hunan provinceNatural Science Foundation of Hunan Province [2016JJ5003]

机构署名：

本校为第一且通讯机构

院系归属：

化学化工学院

摘要：

The base-free O-difluoromethylation of 1,3-diones with difluorocarbene generated from difluoromethylene phosphobetaine (Ph3P+CF2CO2-) is described. The convenient reactions proceeded smoothly to give difluoromethyl enol ethers in moderate to good yields. (C) 2016 Else...

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Base-free O-difluoromethylation of 1,3-diones with difluorocarbene

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