In his paper, the PAN-PVA blend film was prepared by casting process. We investigated a series of factors such as the mass ratio of PAN to PVA, drying temperature of forming membrane and concentration of forming membrane which effect properties of blend film. Tensile strength at break and elongation at break were determinated. The blend films that have high conductivity, good mechanics properties and be suited to eleetromagnetie wave shielding materials were prepared. We had got the optimum condi- tions PAN-PVA blend membrane:the mass fraction...