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Electroextraction of gadolinium from Gd2O3 in LiCl–KCl–AlCl3 molten salts

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成果类型:
期刊论文
作者:
Liu, Kui;Liu, Ya-Lan;Yuan, Li-Yong;Zhao, Xiu-Liang;Chai, Zhi-Fang*;...
通讯作者:
Chai, Zhi-Fang
作者机构:
[Liu, Ya-Lan; Yuan, Li-Yong; Liu, Kui; Chai, Zhi-Fang; Shi, Wei-Qun] Chinese Acad Sci, Inst High Energy Phys, Key Lab Nucl Analyt Tech, Grp Nucl Energy Nanochem, Beijing 100049, Peoples R China.
[Liu, Kui; Zhao, Xiu-Liang] Univ South China, Sch Nucl Sci & Technol, Hengyang 421000, Peoples R China.
[Chai, Zhi-Fang] Soochow Univ, Sch Radiol & Interdisciplinary Sci, Suzhou 215123, Peoples R China.
通讯机构:
[Chai, Zhi-Fang] C
Chinese Acad Sci, Inst High Energy Phys, Key Lab Nucl Analyt Tech, Grp Nucl Energy Nanochem, Beijing 100049, Peoples R China.
语种:
英文
关键词:
Molten chloride;Gadolinium;AlCl3;Intermetallic compounds;Co-reduction
期刊:
Electrochimica Acta
ISSN:
0013-4686
年:
2013
卷:
109
页码:
732-740
基金类别:
Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [91226201]; Chinese Academy of SciencesChinese Academy of Sciences [XDA03010401, XDA03010403, XDA03010404]
机构署名:
本校为其他机构
院系归属:
核科学技术学院
摘要:
This work concerns directly the extraction of gadolinium from Gd 2O3by co-reduction with Al3+in theLiCl-KCl-AlCl3molten salts on the molybdenum and aluminum electrode, respectively, at temperatureof 773 K. Gibbs energy calculation shows that AlCl3 can favorably chloridize Gd2O3and release Gd3+ions. The electrochemical behaviors of Al3+, Gd3+ and the mechanisms of alloy formation were investi-gated by conducting a series of electrochemical techniques. Four typical signals were observed in cyclicvoltammetry, square wave voltammetry and chronopote...

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